All heated objects are allowed to attain,..., before you attempt to weigh them
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As part of the procedure for the determination of the sulfate content of an unknown sample it will be necessary to accurately determine the empty weights of a set of crucibles. This is accomplished by first cleaning the crucible and then heating them in the flame of a Tirrel burner. They are then cooled and weighed. This process of heating and cooling is repeated until successive weighings agree to within 0.2mg. The procedure will, in addition, acquaint the student with the use of the analytical balance and the proper use of the desiccator. Be sure that you read the appendix section dealing with the use of desiccator.
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