dibal h reduction of carboxylic acid
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Temhedmn L.&em, Vol. 34, No. 9, pp. 1491-1494.1993 Printed in Great Britain oo40-4039/93 56.00 + .oo Pergamm Press IAd First General Synthesis of Monosilyl Acetals. Trimethylsilyl Trapping of the Intermediate in DIBALII Reduction of Carboxylic Acid Esters using Trimethylsilyl Trifluoromethanesulfonatel Syun-ichi KIYOOKA.* Masashi SHIROUCHI. and Yuichi KANEKO Department of Chanistry, Kochi University, Akebono-rho. Kochi 780. Japan Key Wordr: Monoaiiyl metal; DIBALH reduction inteamediak Abstract: 'The intemediate g-ted by the DIBALH
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DIBAL is a bulky aluminum hydride reagent that is useful for reducing esters down to aldehydes.
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