discuss the preparation and chemical reactions of acylhalides.
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Acyl halides are reactive compounds that are commonly used as reagents for derivatization of other analytes. The derivatization of acyl halides as analytes can be done using a hydrolysis followed by subsequent derivatization of the acid. Some examples of direct derivatization of the acyl halide are also known. Phosgene can be derivatized using reagents such as 1-(2-pyridyl)piperazine [690] or tryptamine [691] followed by HPLC analysis. Solutions of acyl halides have been analyzed using derivatization on a polymer-immobilized 8-amino-2-naphthoxide [692], reaching a limit of detection of 0.84−1.5 ppb when using HPLC analysis with UV detection at 214 nm.
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