Electrochemical aspect of nitrobenzene reduction
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potentiostatic electrodeposition strategy and employed for the electrochemical reduction of nitrobenzene (NB). First, the .
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Nitrobenzene was reduced electrochemically at a mercury cathode at various controlled potentials in acid electrolytes. Potential control to ±1 mv. was achieved by use of a recently developed instrument which is capable of supplying the high currents required to obtain sufficient quantities of product to make a complete analysis of the product mix. Of nine possible products, only four were obtained in measurable quantities. The composition of the product mix is a sensitive function of both the potential and length of electrolysis.
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