Homogenization process in cast materilas
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let us take alluminium alloy as an example
The evolution of the eutectic structures in the as-cast and homogenized 7X50 aluminum alloys was studied by scanning electron microscopy (SEM), transmission electron microscopy (TEM), energy dispersive spectrometer (EDS), differential scanning calorimetry(DSC), X-ray diffraction(XRD) and tensile test. The results show that the main phases are S(Al2CuMg), T(Al2Mg3Zn3) and MgZn2, with a small amount of Al7Cu2Fe and Al3Zr in the as-cast 7X50 alloy. The volume fraction of the dendritic-network structure and residual phase decreases gradually during the homogenization. After homogenization at 470 °C for 24 h and then 482 °C for 12 h, the T(Al2Mg3Zn3) phase disappears and minimal S(Al2CuMg) phase remains, while almost no change has happened for Al7Cu2Fe. There is a strong endothermic peak at 477.8 °C in the DSC curve of as-cast alloy. A new endothermic peak appears at 487.5 °C for the sample homogenized at 470 °C for 1 h. However, this endothermic peak disappears after being homogenized at 482 °C for 24 h. The T(Al2Mg3Zn3) phase cannot be observed by XRD, which is consistent with that T phase is the associated one of S(Al2CuMg) phase and MgZn2 phase. The volume fraction of recrystallized grains is substantially less in the plate with pre-homogenization treatment. The strength and fracture toughness of the plate with pre-homogenization treatment are about 15 MPa and 3.3 MPa·m½ higher than those of the material with conventional homogenization treatment.
The evolution of the eutectic structures in the as-cast and homogenized 7X50 aluminum alloys was studied by scanning electron microscopy (SEM), transmission electron microscopy (TEM), energy dispersive spectrometer (EDS), differential scanning calorimetry(DSC), X-ray diffraction(XRD) and tensile test. The results show that the main phases are S(Al2CuMg), T(Al2Mg3Zn3) and MgZn2, with a small amount of Al7Cu2Fe and Al3Zr in the as-cast 7X50 alloy. The volume fraction of the dendritic-network structure and residual phase decreases gradually during the homogenization. After homogenization at 470 °C for 24 h and then 482 °C for 12 h, the T(Al2Mg3Zn3) phase disappears and minimal S(Al2CuMg) phase remains, while almost no change has happened for Al7Cu2Fe. There is a strong endothermic peak at 477.8 °C in the DSC curve of as-cast alloy. A new endothermic peak appears at 487.5 °C for the sample homogenized at 470 °C for 1 h. However, this endothermic peak disappears after being homogenized at 482 °C for 24 h. The T(Al2Mg3Zn3) phase cannot be observed by XRD, which is consistent with that T phase is the associated one of S(Al2CuMg) phase and MgZn2 phase. The volume fraction of recrystallized grains is substantially less in the plate with pre-homogenization treatment. The strength and fracture toughness of the plate with pre-homogenization treatment are about 15 MPa and 3.3 MPa·m½ higher than those of the material with conventional homogenization treatment.
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