Question

How to prepare ammonium chloride ammonium hydroxide buffer?

Answer 1

here is your answer mate :-

Ammonia-Ammonium Chloride Buffer: Dissolve 67.5 g of ammonium chloride in about 200 ml of water, add 570 ml of strong ammonia solution and dilute with water to 1000 ml. Ammonia Buffer pH 9.5: Dissolve 33.5 g of ammonium chloride in ISO ml of water, and 42 ml of 10M ammonia and dilute with water to 250 ml.

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Answer 2

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NH4OH, being a weak base, ionizes to a less extent while NH4Cl being a strong electrolyte ionizes almost completely. When a small amount of strong acid like HCl is added, the H+ ions combines with OH- to form un-dissociated water molecules. However, to maintain Ka constant, NH4OH dissociates more thus removing H+ ions.

This buffer is also called Ammoniacal Buffer, Dissolve 90 g of ammonium chloride in 375 mL of 28–30% ammonium hydroxide, and dilute to 500 mL with water. (The pH of a 1 + 10 dilution with water should be about 10.)

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