how to prepare sulphur hexafluoride
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It's synthesized by direct reaction of sulfur and fluorine, so in effect, you can't make it without very specialized equipment. The other concern is disulfur decafluoride, which forms under the same conditions and is highly toxic. The way it is dealt with though is by heating the gas to decompose any disulfur decafluoride and then reacting with sodium hydroxide to get rid of any sulfur tetrafluoride formed.
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