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Weigh 1.260 g of oxalic acid crystals and dissove them in water to prepare 500 ml of M/50 oxalic acid solution using a 500 ml measuring flask. Rinse the pipette with the M/50 oxalic acid solution and pipette out 20 ml of it in a washed titration flask.
Rinse and fill the burette with M/100 KMnO4 solution.
Add one test-tube (~ 20 ml) full of dilute sulphuric acid (~ 2 M) to the solution in titration flask.
Note the initial reading of the burette.
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