preparation of picramide
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PREPARATION OF PICRAMIDE. The method of Kym for conversion of phenols into aromatic amines has been applied to picric acid. An 88% yield of picramide has been obtained by adjusting the reaction temperature to 173 °C., the molar urea: picric acid ratio to 3:1, and the reaction time to 36 hr.
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The method of Kym for conversion of phenols into aromatic amines has been applied to picric acid. An 88% yield of picramide has been obtained by adjusting the reaction temperature to 173 °C., the molar urea: picric acid ratio to 3:1, and the reaction time to 36 hr.
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