Chemistry, asked by yogiiii9216, 1 year ago

Prepare the double salt patash alum and submit for inspection

Answers

Answered by 151500
0

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151500: hope u understand.
Answered by alinakincsem
0
Procedure:

Clean a small piece of scrap aluminum with steel wool and cut it into very small pieces. Aluminium foil may be taken instead of scrap aluminum.

Put the small pieces of scrap aluminum or aluminum foil (about 1.00g) into a conical flask and add about 50 ml of 4 M KOH solution to dissolve the aluminum.

The flask may be heated gently in order to facilitate dissolution.  Since during this step hydrogen gas is evolved this step must be done in a well-ventilated area. Continue heating until all of the aluminum reacts.

Filter the solution to remove any insoluble impurities and reduce the volume to about 25 ml by heating.Allow the filtrate to cool. Now add slowly 6 M H2SO4 until insoluble Al(OH)3 just forms in the solution.

Gently heat the mixture until the Al(OH)3 precipitate dissolves. Cool the resulting solution in an ice-bath for about 30 minutes whereby alum crystals should separate out.  

For better results, the solution may be left overnight for crystallization to continue. In case crystals do not form the solution may be further concentrated and cooled again.

  Filter the crystals from the solution using a vacuum pump, wash the crystals with 50/50 ethanol-water mixture. Continue applying the vacuum until the crystals appear dry.  

Hope this will help you.
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