State two precautions required to ensure accurate results for finding the melting point of a solid
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The melting point of an organic solid can be determined by introducing a tiny amount into a small capillary tube, attaching this to the stem of a thermometer centred in a heating bath, heating the bath slowly, and observing the temperatures at which melting begins and is complete.
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1. The lower end of capillary tube and thermometer should be at same level.
2. The powdwered substance should be uniformly filled in tube so that their is no air gaps.
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