Typical procedure: 37g butanol, 60 g glacial acetic acid and 3 drops of h2so4 are mixed together. The reaction mixture is then poured into 250 cm3 water. The organic layer is separated and washed again with water (100 cm3 ), saturated nahco3 (25 cm3 ) and more water (25 cm3 ). The crude ester is then dried over anhydrous na2so4 (5 g), and then distilled. Yield = 40 g (69 %).
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ummmmmmm. 25 or 556 don't know
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