Write the procedure for preparation of magnesium trisilicate test solution for
chloride limit test I.P.
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Procedure:
Test sample Standard compound
Specific weight of compound is dissolved in water or solution is prepared as directed in the pharmacopoeia and transferred in Nessler cylinder Take 1ml of 0.05845 % W/V solution of sodium chloride in Nessler cylinder
Add 1ml of nitric acid Add 1ml of nitric acid
Dilute to 50ml in Nessler cylinder Dilute to 50ml in Nessler cylinder
Add 1ml of AgNO3 solution Add 1ml of AgNO3 solution
Keep aside for 5 min Keep aside for 5 min
Observe the Opalescence/Turbidity Observe the Opalescence/Turbidity
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