How is anisole prepared?
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Preparation. Anisole is prepared by methylation of sodium phenoxide with dimethyl sulfate or methyl chloride: 2 C6H5O−Na+ + (CH3O)2SO2 → 2 C6H5OCH3 + Na2SO.
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Anisole can be prepared from phenol or its salts by the use of the following methylating agents: methyl chloride;1 sodium methyl sulfate;2 methyl alcohol in the presence of thorium oxide;3 methyl alcohol and β-naphthalenesulfonic acid4 or potassium hydrogen sulfate5 or boron fluoride;6 dimethyl sulfate;7 and methyl
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