How to do crystallize twice from methanol in organic synthesis?
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Crystallization (or recrystallization) is the most important method for purification of organic compounds. The process of removing impurities by crystallization involves dissolving a compound in an appropriate hot solvent, allowing the solution to cool and become saturated with the compound being purified, allowing it to crystallize out of the solution, isolating it by filtration, washing its surface with cold solvent to remove residual impurities, and drying.
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